Glass

2019 年 8 月 20 日

A glass slide randomly picked up in the laboratory.

A Glass Slide
Report
Created on:2019-06-23 23:55:49
Operator:Phil Wu
File
File name:C:\Users\Phil Wu\Documents\Data and Analysis\XRD\XPert\2019June13_Measurement_Hualien Rock Samples\absolute scan_sample3.xrdml
Checksum:011BFB042372D891AE0C1FB52D641874
File size (bytes):13275
Time stamp
Started:2019-06-14 02:56:26
Finished:2019-06-14 03:06:50
Total time (h:m:s):00:10:24
Comment
Configuration=PW3071/xx Bracket, Owner=User-1, Creation date=2014/5/21 ?? 09:08:56
Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001; Minimum step size Omega:0.001
Sample stage=PW3071/xx Bracket
Diffractometer system=XPERT-3
Measurement program=C:\PANalytical\Data Collector\Programs\absolute scan.xrdmp, Identifier={128158DF-6E82-44E4-AF97-6F8E23A28BE0}
Status
Completed
Sample
Sample type:To be analyzed
Measurement type
Single scan
Used wavelength
Intended wavelength type:Kα1
Kα1 (Å):1.540598
Kα2 (Å):1.544426
Kα2/Kα1 intensity ratio:0.50
Kα (Å):1.541874
Kβ (Å):1.392250
Incident beam path
Radius (mm):240.0
X-ray tube 
Name:Empyrean Cu LFF HR (9430 033 7310x) DK402428
Anode material:Cu
Voltage (kV):45
Current (mA):40
Focus 
Focus type:Line
Length (mm):12.0
width (mm): 0.4
Take-off angle (°): 6.0
Filter 
Name:Beta-filter Nickel
Material:Ni
Thickness (mm):0.020
Soller slit 
Name:Soller slits 0.04 rad.
Opening (rad.):0.04
Mask 
Name:Fixed incident beam mask 10 mm
Width (mm):6.60
Anti-scatter slit 
Name:Fixed slit 1/2°
Type:Fixed
Height (mm):0.76
Divergence slit 
Name:Fixed slit 1/4°
Distance to sample (mm):140
Type:Fixed
Height (mm):0.38
Angle (°):0.2177
Diffracted beam path
Radius (mm):240.0
Anti-scatter slit 
Name:Fixed slit 1/4°
Type:Fixed
Height (mm):0.38
Soller slit 
Name:Soller slits 0.04 rad.
Opening (rad.):0.04
Detector 
Name:X’Celerator detector
Type:RTMS detector
PHD – Lower level (%):37.5
PHD – Upper level (%):79.5
Mode:Scanning
Active length (°):2.122
Source
Created by:IOP
Application SW:Data Collector
vs. 4.4a
Instrument control SW:XPERT-3
vs. 7.0/ 20131101
Instrument ID:0000000011156094
Sample mode
Reflection
Scan
Start time stamp:2019-06-14 02:56:26
End time stamp:2019-06-14 03:06:50
Scan axis:Gonio
Scan range (°):  5.0000 – 89.9935
Start position (°):  5.0167 
End position (°): 89.9768 
Step size (°):  0.0334
No. of points:2543
Scan mode:Continuous
Counting time (s):29.845
2\theta scan of a sample holder made of glass.

The measurement indicates material is amorphous = no identified x-ray peaks, in other words the glass is glassy.