Report
Created on: 2019-10-23 10:23:00
Operator: Phil Wu
File
File name: C:\Users\Phil Wu\Documents\Data and Analysis\XRD\XPert\2019May3_Measurement_Hualien Rock Samples\absolute scan_spot scan check.xrdml
Checksum: 473CA3D4865EFFFB95241E76B570A39A
File size (bytes): 9663
Time stamp
Started: 2019-05-04 01:56:55
Finished: 2019-05-04 01:59:27
Total time (h:m:s): 00:02:32
Comment
Configuration=PW3071/xx Bracket, Owner=User-1, Creation date=2014/5/21 ?? 09:08:56
Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001; Minimum step size Omega:0.001
Sample stage=PW3071/xx Bracket
Diffractometer system=XPERT-3
Measurement program=C:\PANalytical\Data Collector\Programs\absolute scan.xrdmp, Identifier={5CE1B059-EF2B-4C44-AE9A-BF0456301CE4}
Status
Completed
Sample
Sample type: To be analyzed
Measurement type
Single scan
Used wavelength
Intended wavelength type: Kα1
Kα1 (Å): 1.540598
Kα2 (Å): 1.544426
Kα2/Kα1 intensity ratio: 0.50
Kα (Å): 1.541874
Kβ (Å): 1.392250
Incident beam path
Radius (mm): 240.0
X-ray tube
Name: Empyrean Cu LFF HR (9430 033 7310x) DK402428
Anode material: Cu
Voltage (kV): 45
Current (mA): 40
Focus
Focus type: Line
Length (mm): 12.0
width (mm): 0.4
Take-off angle (°): 6.0
Filter
Name: Beta-filter Nickel
Material: Ni
Thickness (mm): 0.020
Soller slit
Name: Soller slits 0.04 rad.
Opening (rad.): 0.04
Mask
Name: Fixed incident beam mask 10 mm
Width (mm): 6.60
Anti-scatter slit
Name: Fixed slit 1/2°
Type: Fixed
Height (mm): 0.76
Divergence slit
Name: Fixed slit 1/4°
Distance to sample (mm): 140
Type: Fixed
Height (mm): 0.38
Angle (°): 0.2177
Diffracted beam path
Radius (mm): 240.0
Anti-scatter slit
Name: Fixed slit 1/4°
Type: Fixed
Height (mm): 0.38
Soller slit
Name: Soller slits 0.04 rad.
Opening (rad.): 0.04
Detector
Name: X’Celerator detector
Type: RTMS detector
PHD – Lower level (%): 37.5
PHD – Upper level (%): 79.5
Mode: Scanning
Active length (°): 2.122
Source
Created by: IOP
Application SW: Data Collector
vs. 4.4a
Instrument control SW: XPERT-3
vs. 7.0/ 20131101
Instrument ID: 0000000011156094
Sample mode
Reflection
Scan
Start time stamp: 2019-05-04 01:56:55
End time stamp: 2019-05-04 01:59:27
Scan axis: Gonio
Scan range (°): 4.9980 – 90.0249
Start position (°): 5.0231
End position (°): 89.9999
Step size (°): 0.0501
No. of points: 1696
Scan mode: Continuous
Counting time (s): 10.160
